Isothermal Oxidation Behavior of Ferritic Oxide Dispersion Strengthened Alloy at High Temperatures

Eddy Agus Basuki; Nickolas Adrianto; Rahmadhani Triastomo; Akhmad Ardian Korda; Tria Laksana Achmad; Fadhli Muhammad; Djoko Hadi Prajitno

doi:10.5614/j.eng.technol.sci.2022.54.2.10

Authors

Eddy Agus Basuki Department of Metallurgical Engineering, Faculty of Mining and Petroleum Engineering, Institut Teknologi Bandung, Jalan Ganesa No. 10 Bandung 40132,
Nickolas Adrianto Department of Metallurgical Engineering, Faculty of Mining and Petroleum Engineering, Institut Teknologi Bandung, Jalan Ganesa No. 10 Bandung 40132,
Rahmadhani Triastomo Department of Metallurgical Engineering, Faculty of Mining and Petroleum Engineering, Institut Teknologi Bandung, Jalan Ganesa No. 10 Bandung 40132,
Akhmad Ardian Korda Department of Metallurgical Engineering, Faculty of Mining and Petroleum Engineering, Institut Teknologi Bandung, Jalan Ganesa No. 10 Bandung 40132,
Tria Laksana Achmad Department of Metallurgical Engineering, Faculty of Mining and Petroleum Engineering, Institut Teknologi Bandung, Jalan Ganesa No. 10 Bandung 40132,
Fadhli Muhammad Department of Metallurgical Engineering, Faculty of Mining and Petroleum Engineering, Institut Teknologi Bandung, Jalan Ganesa No. 10 Bandung 40132,
Djoko Hadi Prajitno Nuclear Technology Center for Materials and Radiometry, National Atomic Agency of Indonesia, Jalan Tamansari No. 71, Bandung 40132

DOI:

https://doi.org/10.5614/j.eng.technol.sci.2022.54.2.10

Keywords:

ferritic steel, interdiffusion, isothermal oxidation, mechanical alloying, oxide dispersion strengthening

Abstract

This paper discusses the oxidation behaviors of ODS steel alloy of Fe-16Cr-4Al-1Ni-0.4ZrO₂ at 700?, 800?, and 900?. X-ray diffraction (XRD) as well as X-ray mapping in a scanning electron microscope were used to characterize the oxidation behavior of the samples. The rate of oxidation was measured based on the thickness of the oxide formed on the surface of the samples. Six types of oxides were identified in all ODS Fe-16Cr-4Al-1Ni-0.4ZrO₂ alloy samples after the oxidation tests, dominated by Fe₂O₃, Fe₃O₄, Cr₂FeO₄, AlFeO₃, Al₂FeO₄, and AlFe₂O₄. The oxidation kinetics of ODS Fe-16Cr-4Al-1Ni-0.4ZrO₂ steel at 700, 800, and 900? followed logarithmic oxidation rate behavior.

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References

International Atomic Energy Agency, Climate Change and Nuclear Power 2018, Vienna: International Atomic Energy Agency, 2018.

Arostegui, D.A. & Holt, M., CRS Report, Advanced Nuclear Reactors: Technology Overview and Current Issues, Congressional Research Service, https://crsrepoerts.congress.gov, R45706, April 18, 2019.

Klueh, R.L., Oxide Dispersion Strengthened Steels: A Comparison of Some Commercial and Experimental Alloys, Journal of Nuclear Materials, 341, pp. 103-114, 2005.

Zinkle, S.J. & Snead, L.L., Designing Radiation Resistance in Materials for Fusion Energi, Annual Review of Materials Research, 44(1), pp. 241-267, 2014.

Rebak, R.B., Terrani, K.A., Gassmann, W.P., Williams, J.B. & Ledford, K.L., Improving Nuclear Power Plant Safety with FeCrAl Alloy Fuel Cladding, MRS Advances, 2(21-22) (Energy and Sustainability), pp. 1217-1224, 2017.

Gupta, V.K., Larsen, M. & Rebak, R.B., Utilizing FeCrAl Oxidation Resistance Properties in Water, Air and Steam for Accident Tolerant Fuel Cladding, ECS Trans., 85(2), pp. 3-12, 2018. DOI: 10.1149/08502. 0003ecst.

Enkvist, J., Bexell, U., Grehk, M. & Olsson, M., High Temperature Oxidation of FeCrAl-alloys - Influence of Al-concentration on Oxide Layer Characteristics, Materials and Corrosion, 60(11), pp. 876-881, 2009.

Birks, N. & Meier G.H., Introduction to High Temperature Oxidation of Metals, London, Edward Arnold, 1983.

Issartel, C., Buscail, H., Chevalier, S. & Favergeon, J., Effect of Yttrium as Alloying Element on a Model Alumina-Forming Alloy Oxidation at 1100?, Oxidation of Metals, 80, pp. 409-420, 2017.

Benz, H.U. & Zoz, H., Nanostructured Ferritic Alloys (NFA) as the Next Generation ODS Manufactured by High Kinetic Processing (HKP), The 4th International Conference on Powder Metallurgy in Asia, Hsinchu, Taiwan, Apr. 09-11, 2017.

Kumar, P.K., Sai, N.P. & Krishna, A.G., Effect of Y2O3 and ZrO2 on the Microstructure and Mechanical Properties of Nano-ODS 21Cr-9Mn-6Ni Steels, Materials and Technology, 52(4), pp. 493-497, 2018.

Raghavendra, K., Dasgupta, A., Bhaskar, P., et al., Synthesis and Characterization of Fe-15wt.% ZrO2 Nanocomposite Powders by Mechanical Milling, Powder Technology, (287), pp. 190-200, 2015.

Li, S., Zhou, Z., Wang, M., Hu, H., Zou, L., Zhang, G. & Zhan, L., Microstructure and Mechanical Properties of 16Cr-ODS Ferritic Steel for Advanced Nuclear Energy System, Journal of Physics: Conference Series 419, 012036, 201. DOI:10.1088/1742-6596/419/1/012036.

Wang, C., Luo, J., Guo, N., Tu, J., Ye, H., Zhang, P. & Yan, Q., Effect of Yttrium Contents on the Microstructure of a Hot-Rolled Tantalum-Containing 12Cr-ODS Steel, Frontiers in Materials, 11 December 2019, DOI: 10.3389/fmats.2019.00317.

Silalahi, M, Bandriyana, B., Ahda, S., Sugeng, B. & Dimyati, A., Synthesis and Characterization of High Chromium Zirconia Oxide Dispersion Strengthened (ODS) Steel, IOP Conf. Series: Journal of Physics: Conf. Series 1436, 012055, 2020. DOI:10.1088/1742-6596/1436/1/012055.

Khanna, A.S., High-Temperature Oxidation in Handbook of Environmental Degradation of Materials, Third Edition, M. Kutz (ed.), Elsevier Inc., pp. 3-25, 2018.

Narita, T. & Hayashi, S., Internal Oxidation and Nitridation Behavior of an Fe-5 mass?Al Alloy at 1073 K, Journal Japan Institute of Metals, 63(10), pp. 1311-1316, 1999.

Junceda, A.G., Rodriguez, N.G. & Campos, M., Effect of Zirconium on the Microstructure and Mechanical Properties of an Al-Alloyed ODS Steel Consolidated by FAHP, Journal American Ceramic, 11(98), pp. 3582-3587, 2015.

Chen, Z., Wang, L., Li, F. & Chou, K., Thermodynamic Analysis of the Corrosion of Fe-16Cr Alloy Interconnect of Solid Oxide Fuel Cell under Various Atmospheres, High Temperature Material Processing, 33(5), pp. 439-445, 2014.

Liang, T., Li, Y., Ao, R., Zhang, X. & Zeng, J., On the Oxidation Resistance of the Compound Fe-based Protective Coating by Supersonic Arc Spraying at 1123 K, Proceeding of The Asia Pacific Engineering and Technology Conference, pp. 604-610, 2017.